分析化学实验-(英汉双语版)

前言Chapter 1 Basic Knowledge of Analytical Chemistry Experiments 1.1 Basic Requirements for Analytical Chemistry Experiments 1.2 Basic Knowledge of the LaboratoryChapter 2 Basic Operation for Quantitative Analysis 2.1 Analytical Balance 2.2 Pipetting and Constant Volume Operation 2.3 Burette and Basic Operations for Titration Analysis 2.4 Basic Operations of Gravimetric AnalysisChapter 3 Quantitative Analysis Experiments 3.1 Basic Operation Practices Exp.1 Practices of Analytical Balance Exp.2 Practices of Basic Operation for Titration Analysis 3.2 Acid-base Titration Experiments Exp.3 Preparation and Standardization of NaOH Standard Solution Exp.4 Preparation and Standardization of HCl Solution Exp.5 Determination of Boric Acid in Food Additives Exp.6 Analysis of Mixed Alkali Exp.7 Determination of Nitrogen in Ammonium Salts Exp.8 Determination of Total Phosphorus in Phosphate Fertilizer Exp.9 Determination of Total Acidity in Edible Vinegar Exp.10 Determination of the Molar Mass of Organic Acids 3.3 Complexometric Titration Experiments Exp.11 Preparation and Standardization of EDTA Standard Solution and Determination of Water Hardness Exp.12 Determination of Calcium and Magnesium in Industrial Raw Materials Exp.13 Determination of Pb2+ and Bi3+ in Mixture of Pb2+ and Bi3+ Exp.14 Determination of Aluminum and Magnesium in Gastropine Tablet Exp.15 Determination of EDTA in Detergents Exp.16 Determination of Iron, Aluminum, Calcium and Magnesium in Cement Clinker Exp.17 Determination of Aluminum in Industrial Aluminum Sulfate 3.4 Redox Titration Experiments Exp.18 Preparation and Standardization of Potassium Permanganate Standard Solution and Determination of H2O2 Exp.19 Determination of Iron in Iron Ore by Potassium Dichromate Method (Mercury-Free Method) Exp.20 Determination of Chemical Oxygen Demand in Environmental WaterSamples (KMnO4 Method) Exp.21 Determination of Chemical Oxygen Demand in Sewage (K2Cr2O7 Method) Exp.22 Determination of Copper in Copper Salt by Indirect Iodimetry Exp.23 Determination of Calcium in Calcium Preparations Exp.24 Determination of Dissolved Oxygen in Water Exp.25 Determination of Vitamin C in Juice Exp.26 Determination of Glucose in Glucose Injection 3.5 Precipitation Titration and Gravimetric Analysis Experiments Exp.27 Determination of Chlorine in Soluble Chloride by Mohr Method Exp.28 Determination of Chlorine in Soluble Chloride by Vollhard Method Exp.29 Determination of Barium in Barium Salt by Gravimetric Method Exp.30 Determination of Barium in Barium Salts (Microwave Drying Gravimetric Method) Exp.31 Determination of Potassium in Fertilizer Exp.32 Determination of Nickel in SteelChapter 4 Spectrophotometry and Common Separation Methods Experiments Exp.33 Spectrophotometric Determination of Iron with Phenanthroline Exp.34 Determination of NO2– in Food Exp.35 Determination of Available Phosphorus in Soil Exp.36 Determination of Total Flavonoids in Bamboo Leaves by Spectrophotometry Coupled with Microwave-assisted Extraction Technique Exp.37 Determination of Trace Lead in Environmental Water Samples by Extraction Separation-spectrophotometry Exp.38 Separation and Identification of Amino Acids by Paper Chromatography Exp.39 Separation of Food Pigments by Paper ChromatographyChapter 5 Comprehensive Design Experiments 5.1 Acid-base Titration Design Experiments Exp.40 Determination of SiO2 by Potassium Fluosilicate Method Exp.41 Determination of NaHCO3 and Na2CO3 in Biscuits Exp.42 Determination of Boron Trioxide of Slag 5.2 Complexometric Titration Design Experiments Exp.43 Determination of ZnO in Calamine Lotion Exp.44 Determination of Nickel and Magnesium in Nickel-magnesium Alloys Exp.45 Determination of Each Component in Mixture of Mg2+ and EDTA 5.3 Redox Titration Design Experiments Exp.46 Determination of Chromium in Alloys Exp.47 Determination of Iodine in Iodized Salt Exp.48 Determination of Ferrous Oxide in Iron-containing Steel Slag 5.4 Precipitation Titration Design Experiments Exp.49 Determination of Sodium Chlorine in Food Exp.50 Determination of Chloride Ion in Complex Fertilizer Exp.51 Determination of Silver in Nylon Silver-plated Fiber 5.5 Spectrophotometry Design Experiments Exp.52 Determination of Chromium and Manganese in Steel by Spectrophotometry Exp.53 Determination of Trace Chlorine in Air Exp.54 Determination of Lead in Plant Leaves by Spectrophotometry 5.6 Comprehensive Experiments Exp.55 Preparation and Composition Determination of Potassium Copper (Ⅱ) Dioxalate Exp.56 Preparation of Sodium Thiosulfate and Determination of Product Content Exp.57 Determination of Zinc Oxide and Boron Trioxide in Flame RetardantsAppendix Appendix 1 Preparation of Commonly Used Buffer Appendix 2 Commonly Used Indicator Appendix 3 Concentrations and Densities of Common Acid-base Solutions Appendix 4 Common Primary Standard and Their Drying Conditions and Applications Appendix 5 Molecular Weight of Common Compounds第1章 分析化学实验基本知识 1.1 分析化学实验的基本要求 1.2 实验室基本知识第2章 定量分析基本操作 2.1 分析天平 2.2 移液和定容操作 2.3 滴定管及滴定分析基本操作 2.4 重量分析法的基本操作第3章 定量分析实验 3.1 基础操作练习 实验1 分析天平称量练习 实验2 滴定分析基本操作练习 3.2 酸碱滴定实验 实验3 NaOH标准溶液的配制和标定 实验4 HCl溶液的配制和标定 实验5 食品添加剂中硼酸含量的测定 实验6 混合碱的分析 实验7 铵盐中氮含量的测定 实验8 磷肥中全磷的测定 实验9 食用醋总酸度的测定 实验10 有机酸摩尔质量的测定 3.3 络合滴定实验 实验11 EDTA标准溶液的配制、标定和水硬度的测定 实验12 工业原料中钙、镁含量的测定 实验13 铅、铋混合溶液中铅、铋含量的测定 实验14 胃舒平片中铝和镁含量的测定 实验15 洗涤剂中EDTA含量的测定 实验16 水泥熟料中铁、铝、钙、镁含量的测定 实验17 工业硫酸铝中铝含量的测定 3.4 氧化还原滴定实验 实验18 高锰酸钾标准溶液的配制、标定和H2O2含量的测定 实验19 重铬酸钾法测定铁矿石中的铁含量（无汞法） 实验20 环境水样中化学需氧量的测定（KMnO4法） 实验21 污水中化学需氧量的测定（K2Cr2O7法） 实验22 间接碘量法测定铜盐中的铜含量 实验23 钙制剂中钙含量的测定 实验24 水中溶解氧的测定 实验25 果汁中维生素C含量的测定 实验26 葡萄糖注射液中葡萄糖含量的测定 3.5 沉淀滴定及重量分析法实验 实验27 莫尔法测定可溶性氯化物中的氯含量 实验28 福尔哈德法测定可溶性氯化物中的氯含量 实验29 重量分析法测定钡盐中的钡含量 实验30 钡盐中钡含量的测定（微波干燥重量法） 实验31 肥料中钾含量的测定 实验32 钢铁中镍含量的测定第4章 分光光度法及常用分离方法实验 实验33 邻二氮菲分光光度法测定铁 实验34 食品中NO2-含量的测定 实验35 土壤中有效磷的测定 实验36 微波辅助萃取-分光光度法测定竹叶中总黄酮 实验37 萃取分离-分光光度法测定环境水样中微量铅 实验38 纸色谱法分离和鉴定氨基酸 实验39 纸色谱法分离食用色素第5章 综合设计实验 5.1 酸碱滴定设计实验 实验40 氟硅酸钾法测定SiO2 实验41 饼干中NaHCO3和Na2CO3含量的测定 实验42 矿渣中三氧化二硼的测定 5.2 络合滴定设计实验 实验43 炉甘石洗剂中ZnO含量的测定 实验44 镍镁合金中镍、镁的测定 实验45 Mg2+-EDTA混合液中各组分的测定 5.3 氧化还原滴定设计实验 实验46 合金中铬含量的测定 实验47 加碘食盐中碘含量的测定 实验48 含铁钢渣中氧化亚铁含量的测定 5.4 沉淀滴定设计实验 实验49 食品中氯化钠的测定 实验50 复合肥料中氯离子含量的测定 实验51 尼龙镀银纤维中银含量的测定 5.5 分光光度法设计实验 实验52 分光光度法测定钢样中的铬和锰 实验53 空气中微量氯气的测定 实验54 分光光度法测定植物叶中的铅含量 5.6 其他综合实验 实验55 二草酸根合铜（Ⅱ）酸钾的制备及组成测定 实验56 硫代硫酸钠的制备及产物含量的测定 实验57 阻燃剂中氧化锌和三氧化二硼的测定附录 附录1 常用缓冲溶液的配制 附录2 常用指示剂 附录3 常用酸碱溶液的浓度和密度 附录4 常用基准物质及其干燥条件与应用 附录5 常用化合物的分子量主要参考文献