有机化学实验/陈彪/英汉双语教材

Chapter 1Introduction of Experimental Organic Chemistry1 11Basic Rules for the Organic Chemistry Lab1 12Common Lab Equipment and Apparatus2 13General Lab Safety7 14Disposal of Lab Waste9 15Common Organic Solvents9 16Experimental Preview Record and Laboratory Report13 17Chemical Literature14 Reference15 Chapter 2Basic Experimental Techniques17 21Heating and Cooling17 22Drying and Drying Agent17 23Filtration19 24Solvent Extraction and Solution Washing21 25The Purification and Separation of Liquid Organic Substances24 26The Purification and Separation of Solid Organic Substances32 27Chromatographic Techniques38 28The Determination of the Physical Constant of Organic Compound47 Chapter 3Comprehensive Experiment56 Part 1Synthesis56 31Synthesis of Cyclohexene56 32Synthesis of Ethyl Bromide57 33Synthesis of 2chlorobutane (secbutyl chloride)59 34Synthesis of diethyl ether61 35Synthesis of Phenetole (ethyl phenolate)62 36Synthesis of Benzoic Acid and Benzyl Alcohol63 37Synthesis of Acetophenone65 38Synthesis of Benzophenone (Friedel Crafts acylation method)67 39Synthesis of Cyclohexanone69 310Synthesis of Adipic Acid71 311Synthesis of Benzoic Acid73 312Synthesis of Cinnamic Acid74 313Synthesis of Ethyl Acetate76 314Synthesis of Isoamyl Acetate (banana oil)78 315Synthesis of Acetylsalicylic Acid (aspirin)79 316Synthesis of Methyl Salicylate (oil of wintergreen)81 317Synthesis of Ethyl Acetoacetate83 318Synthesis of Acetanilide84 319Synthesis of ptoluidine86 320Synthesis of Anthranilic Acid (2aminobenzoic acid)88 321Synthesis of Phenoxyacetic Acid90 322Synthesis of Methyl Orange92 323Synthesis of Benzocaine94 324Synthesis of Nacetylptoluidine96 325Synthesis of Benzoin96 326Synthesis of 2Nitroresorcinol98 327Synthesis of Quinoline100 328Synthesis of Nikethamide103 329The Reduction of Camphor104 330Synthesis of 3(2,5xylyloxyl) Propyl Chloride and Monitoration of Reaction Process106 Part 2Extraction and Separation107 331The Recrystallization of Benzoic Acid107 332Extraction and Purification of Nicotine109 333Isolation of Caffeine From Tea Leave110 334Isolation of Effective Components from the Citrus112 335Isolation of Benberine from Coptis chinensis Franch114 336Paper Chromatography of Amino Acid115 337Paper Electrophoresis of Amino Acid117 338Separation of Green Leaf Pigments by TLC119 Chapter 4Appendix121 41Experiments from the Literature121 42List of the Elements with Their Symbols and Atomic Masses123 43Main Families of Organic Compounds126 44Boling Point and Density of Some Common Organic Reagents126 第1章有机化学实验基础知识127 11有机化学实验的基本规则127 12常用的玻璃仪器和实验装置127 13有机化学实验的安全知识129 14有机化学实验废物的处置130 15常用有机溶剂及纯化130 16实验预习记录和实验报告134 17有机化学的文献资料134 第2章有机化学实验基本操作136 21加热和冷却136 22干燥与干燥剂136 23过滤137 24萃取和洗涤139 25液体有机化合物的分离与纯化142 26固体有机化合物的提纯147 27色谱法151 28有机化合物物理常数的测定156 第3章综合实验163 **部分制备163 31环己烯的制备163 32溴乙烷的制备164 332氯丁烷的制备165 34乙醚的制备166 35苯乙醚的制备167 36苯甲醇和苯甲酸的制备168 37苯乙酮的制备169 38二苯甲酮（酰基化法）的制备171 39环己酮的制备172 310己二酸的制备173 311苯甲酸的制备175 312肉桂酸的制备176 313乙酸乙酯的制备177 314乙酸异戊酯的制备（香蕉油）178 315乙酰水杨酸的制备（阿司匹林）180 316水杨酸甲酯的制备（冬青油）181 317乙酰乙酸乙酯的制备182 318乙酰苯胺的制备183 319对甲苯胺的合成184 320邻氨基苯甲酸的合成185 321苯氧乙酸的制备187 322甲基橙的制备189 323苯佐卡因的制备190 324对甲基N乙酰苯胺的合成192 325安息香的合成192 3262硝基雷琐酚的制备194 327喹啉的制备195 328尼可刹米的制备197 329樟脑的还原反应199 330降血脂药吉非贝齐中间体3（2，5二 甲基苯氧基）1氯丙烷的制备200 第二部分提取、分离与鉴定201 331苯甲酸的提纯201 332烟碱的提取与鉴定202 333从茶叶中提取咖啡因203 334橘皮中有效成分的提取、分离 与鉴定205 335黄连中黄连素的提取及鉴定206 336纸色谱分离鉴定氨基酸208 337纸上电泳分离鉴定氨基酸209 338薄层色谱法分离叶绿素210 参考文献212